Tougaard, Practical Guide to the Use of Backgrounds in Quantitative XPS, J. Shard, Practical Guides for X-Ray Photoelectron Spectroscopy: Quantitative XPS, J.
Free xps peak fitting free#
Powell, Practical Guide for Inelastic Mean Free Paths, Effective Attenuation Lengths, Mean Escape Depths, and Information Depths in x-Ray Photoelectron Spectroscopy, J. Artyushkova, Practical Guide for Curve Fitting in X-Ray Photoelectron Spectroscopy, J. Gengenbach, Practical Guides for X-Ray Photoelectron Spectroscopy: Analysis of Polymers, J. Morgan, Practical Guide for X-Ray Photoelectron Spectroscopy: Applications to the Study of Catalysts, J. Smentkowski, Practical Guides for X-Ray Photoelectron Spectroscopy: First Steps in Planning, Conducting, and Reporting XPS Measurements, J. Roberts, XPS Guide: Charge Neutralization and Binding Energy Referencing for Insulating Samples, J. XPS Guides for Data Acquisition and Analysis
Free xps peak fitting software#
An offline version of ESCape is avalible to all the Supra users in AMCaT upon request.ĬasaXPS is a popular software package for fitting and analyzing XPS data. This is an excellent reference to determine constraints on peak positions when fitting XPS spectra.ĮSCape is the software written By Kratos to acquire and analyze XPS data from the Supra. NIST’s X-ray Photoelectron Spectroscopy Database has an extensive database of binding energies for elements in specific compounds. The website covers general analysis methods as well as element specific discussions on peak shapes and positions. is an excellent resource for analyzing XPS and Auger data. Kratos, the manufacturer of our Axis Supra +. It is available for Windows, Mac, and Linux operating systems.
Free xps peak fitting for free#
The SESSA package can be downloaded for free on the NIST website.
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The simulated data can then be compared against the acquired data. You can specify the composition of your material, specify peak positions based on reference data from similar compounds, and the operating parameters of the spectrometer. Samples can be configured in multiple ways: Multilayers, Islands, wires, spheres on substrates. NIST’s Simulation of Electron Spectra for Surface Analysis (SESSA) is a great tool for simulating your AES XPS Spectra. The proposal was submitted by Professor Kristi Koski, and co-PIs Charles S Fadley, Coleman Kronawitter, Frank Osterloh and Jesus Velazquez. The Axis Supra is also equipped with a high tilt sample arm which can be used to acquire Angle-Resolved XPS (ARXPS).Īcquisition of the Axis Supra was funded by NSF-MRI 182838. Furthermore, the heat and cool holder allow the user to perform in-situ experiments in the sample analysis chamber. The SSS gives the user the in-situ capability of exposing samples to a variety of gas environments pre and post analysis without having to break vacuum. The Axis Supra is also equipped with a Minibeam 4, Ar+ ion gun designed for surface cleaning and relative depth profiling.Īn ultrahigh vacuum (UHV) Surface Science Station (SSS) is attached to the analysis chamber by a load lock. Some library entries also have a single combined peak without a suffix e.g. The option is provided to display both components, or only the major or larger component of the doublet (p3/2, d5/2, f7/2). The Axis Supra is equipped with a Monchromated X-Ray Gun (Al and Ag anodes), an Achromatic X-Ray Gun (Al and Mg anodes), and Ultraviolet Photoelectron Spectroscopy (UPS) He lamp.Ī Hemispherical and Spherical mirror analyzer equipped with a 128 channel Delay-Line Detector allows for fast parallel imaging and excellent signal-to-noise. Doublet Peak Options XPS peaks from p,d and f orbitals have two components creating a doublet. you can use Peak Fit software or Orgin software for peak fitting. XPS is a surface sensitive technique, which allows the user to analyze the composition of their sample within the first 10nm of the surface. You can find free XPS peak fitting software. The Axis Supra is a X-Ray Photoelectron Spectrometer (XPS) manufactured by Kratos Analytical. Because hafnium is a good absorber of neutrons, has superb mechanical and corrosion resistance properties, it is used to make nuclear control rods, such as those used in nuclear submarines.Photo courtesy of Andrew Thron. While found in natural zirconium compounds, hafnium does not exist as a free element in nature. Half of all hafnium metal produced is through a by-product of zirconium refinement.
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Hafnium, a lustrous, silverish gray tetravalent transition metal, has many characteristics similar to that of zirconium. von Hevesy discovered the element hafnium and were also able to predict the electron structure of the element. While using X-ray spectroscopy to study the arrangements of the outer electrons within atoms in samples of zirconium ore, D. Discoverer: Dirk Coster, George von Hevesy